Preparation of alumina nanoshell coated porous silica …

The prepared nanoAl 2 O 3 /mesoSiO 2-5 particles were well dispersed, smooth and highly spherical (Fig. 1).It is even very difficult to find the difference between bare silica and nanoAl 2 O 3 /mesoSiO 2-5 particles in the aspect of shape.This illustrated that the precipitation of alumina nanoshell on the surface of the silica sphere did not cause any aggregation, …

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Separation of aluminum and silica from coal gangue by …

High-temperature direct acid leaching is highly effective for separating metal ions and silica in coal gangue. An increase in temperature significantly improves the extraction …

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Removal of Silica and Alumina as Impurities from Low …

More alumina and silica were removed during magnetic separation followed by flotation process because the iron-silica and iron-alumina aggregated minerals were separated more by their difference in floatability [21] because there are weak magnetic particles and was difficult to separate them during two stage magnetic separation.

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CHAPTER 2 Hydrothermally-Stable Alumina-Silica …

Hydrogen Separation 2.1. Introduction This chapter describes in detail the preparation of hydrothermally-stable silica based membranes. A thin layer of a dual-element alumina-silica composition was deposited on a ... The alumina-silica composite membranes were deposited on macroporous alumina supports by a chemical vapor deposition (CVD ...

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Silica-alumina zeolite adsorbents for oxygen generation via …

Considering that silica-alumina zeolite is predominantly adopted as an adsorbent for equilibrium separation in the field of O 2 generation from air separation, the following review will focus on clarifying the requirements for silica-alumina zeolite …

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Removal of Silica and Alumina as Impurities from …

This study investigates the removal of silica and alumina as impurities from hematite based low-grade iron ore containing 34.18 mass% iron, 31.10 mass% of silica and 7.65 mass% alumina. Wet high-intensity magnetic separation …

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Silica membranes for hydrogen separation prepared by chemical …

1. Introduction1.1. Silica membranes for hydrogen separation. Hydrogen permeable and selective membranes are potentially among the most important inorganic membranes in the gas separation field due to the importance of hydrogen as an industrial feedstock for the production of fuels and many chemicals [1], [2].The membranes have been …

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Abstract and Figures

The separation of alumina and silica from ORCs. obtained at 700–1100 C was conducted by alkaline. leaching in 160 g/L NaOH solution with liquid/solid/ of 50 mL/5 g at 140 ...

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Separation of alumina from aluminum-rich coal fly ash …

Abstract High-alumina coal fly ash (CFA) is considered as an important and cheap resource of aluminum. On account of high valence aluminum often trapped in aluminosilicate basic glassy phase and mullite (Al6Si2O13), efficiently separating aluminum and silicon is an essential precondition for maximizing the recycling of alumina from CFA, which is conducive to …

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US3006723A

the silicate content of the bauxite is most important, for any reactive silica combines with alumina during the digestion with caustic soda and is carried into the red mud as an insoluble sodium aluminum silicate. About 1 pound of alumina and 1 pound of soda are lost for each pound of silicate in the bauxite and these losses have prevented the use of alumina ores containing …

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Efficient separation of alumina and silica in reduction …

Alkali leaching was employed to investigate the separation of alumina and silica in roasted kaolin obtained by roasting kaolin alone in air at 1273 K for 60 min and in clinker prepared by roasting the mixed raw meal of kaolin, ferric oxide and coal powder with Fe 2 O 3 /Al 2 O 3 /C molar ratio of 1.2:2.0:1.2 in reducing atmosphere at 1373 K for 60 min. The thermodynamic …

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Comprehensive Extraction of Silica and Alumina from High-Alumina …

Then, the efficient separation of silica and alumina from the reductively roasted product is achieved by alkaline leaching, because hercynite with spinel structure is stable in alkaline solution. The alumina in hercynite treated by pre-oxidation roasting can be efficiently extracted by Bayer digestion, and hematite in red mud can be recycled by ...

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High-Selectivity, High-Flux Silica Membranes for …

Coherent and strong porous α-Al 2 O 3 membrane supports were made from granulated alumina powder ().The supports were uniaxially pressed at 10 5 kPa to shape the disk, followed by isostatic pressing at 4000 kPa to …

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Hydrothermally stable silica–alumina composite membranes …

The silica–alumina composite membranes were prepared using the previously described γ-alumina multilayer as the substrate by the deposition of a thin silica–alumina layer by the chemical vapor deposition method. ... Sol–gel derived silica membranes for separation of hydrogen at high temperature-separation performance and stability ...

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Efficient separation of silica and alumina in simulated CFB …

After magnetic separation, the alumina content, silica content, and the mass ratio of alumina/silica in the non-magnetic part of the separation product was 80.36 wt%, 6.49 wt%, and 12.38 ...

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An efficient and environmental friendly strategy for alumina …

Efficient separation of silica and alumina in simulated CFB slag by reduction roasting-alkaline leaching process. Waste Manag. (2019) R.H. Lin et al. Application of sequential extraction and hydrothermal treatment for characterization and enrichment of rare earth elements from coal fly ash.

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Catalytic materials based on silica and alumina: Structural features

The structural, surface chemical and catalytic properties of the materials belonging to the SiO 2 Al 2 O 3 system are reviewed critically. In particular, amorphous silicas, transitional aluminas, different silica-aluminas (silica-rich and alumina-rich) and protonic zeolites are taken into consideration.

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Hydrothermally stable silica–alumina composite membranes …

Composite membranes prepared by sol–gel methods composed of silica with other inorganic oxides such as alumina (Al 2 O 3), titania (TiO 2) and zirconia (ZrO 2) have been reported to improve the stability of silica membranes for use under humid atmospheres at high temperature.Fotou et al. [20] introduced these oxides and MgO into the membranes by doping …

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How can you separate alumina from silica in a bauxite are …

Baeyer's process is one of the methods used. Al2O3 is leached out as sodium aluminate (andSiO2) too as sodium silicate) leaving the impurities behind. (b) Now, CO2 gas is passed …

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Electrochemically Enhanced Dissolution of Silica and …

Electrochemically Enhanced Dissolution of Silica and Alumina in ... double layers between the dissimilar charged surfaces at small intersurface separation distances (<1 Debye length). A semiquantitative model shows that overlap of the electric double layers can change the magnitude and direction of the electric

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Comprehensive Extraction of Silica and Alumina from …

alkaline leaching were carried out to realize the separation of silica and alumina in actively roasted product. Subsequently, the alumina in the leaching residue was extracted by Bayer digestion. Experimental Materials The composition of coal gangue used in this study is shown in Table 2. The proximate analysis results indicate

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Extraction of alumina and silica from high-silica bauxite …

In this paper, a novel process is proposed to extract Al2O3 and SiO2 from high-silica bauxite without residue discharge, that is, sintering bauxite with Na2CO3 followed by two-step …

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Column Chromatography (video)

The stationary phase is an adsorbent powder or gel such as silica gel or alumina. Silica gel and alumina are highly polar so they interact strongly with polar compounds and solvents, and weakly with nonpolar molecules. ... To start the separation, add the sample to the column without disturbing the sand. Use small portions of solvent to rinse ...

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Solutions for Light Hydrocarbons and Gases: PLOT …

Alumina Silica Carbon Porous polymers Porous polymers Silica Porous polymers Select Perm. Gases Select Low Sulfur Porous polymers Silica Lowox OxyPLOT 18 July 31, 2014 . ... • Poor C4 isomer separation Alumina preferred • Not sensitive to moisture • Good choice for solvents and CFCs 19 July 31, 2014 .

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Mechanical Activation of Coal Fly Ash for the Improvement of Alumina …

The pre-separation of silica and alumina in aluminosilicates is of great significance for efficiently treating alumina-/silica-bearing minerals for alumina production. In this work, the reaction ...

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Hydrothermally Stable Silica–Alumina Composite Membranes …

Silica-based membranes prepared by chemical vapor deposition of tetraethylorthosilicate (TEOS) on γ-alumina overlayers are known to be effective for hydrogen separation and are attractive for ...

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Separation of aluminum and silica from coal gangue by …

Separation of aluminum and silica from coal gangue by elevated temperature acid leaching for the preparation of alumina and SiC. Author links open overlay panel Jin Xiao, ... Alumina is widely used as a catalyst and adsorbent. It is also used in the production of metallic aluminum. China, as the largest producer of aluminum, requires a large ...

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Silica, alumina and aluminosilicates as solid stationary phases …

It was observed that the silica–alumina solids, except AlSi(8), showed a better separation than alumina and silica. Separation was improved when these samples are thermally treated. In this context, one should refer to the pore structural characteristics of the silica–alumina solids. It was mentioned that silica–alumina have much better ...

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Separation of alumina and silica from metakaolinite by …

The pre-separation of silica and alumina in aluminosilicates is of great significance for efficiently treating alumina-/silica-bearing minerals for alumina production. In this work, the reaction ...

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Efficient separation of silica and alumina in simulated CFB …

As an alkaline leaching method, roasting-leaching process is a potential way to separate silica and alumina in primary alumina-/silica-bearing minerals (Herbert and Hans, …

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Efficient separation of alumina and silica in reduction …

amorphous silica liberated from kaolinite at 980 °C is 66.67% at most. In order to develop a new process for efficiently realizing the separation of alumina and silica in kaolinite, LI et al [17] have introduced ferric oxide- involved reduction roasting process, which involves fully converting kaolinite into hercynite and free silica,

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Mineral phase transformation in coal gangue by high …

On the other hand, some scholars use the caustic separation to extract silicon-containing substances from coal gangue. Caustic separation uses caustic substances such as sodium hydroxide or sodium carbonate to convert the silica-containing substances in the coal gangue into sodium silicate solution, and the alumina-containing substances are enriched in …

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Alumina for Column Chromatography

Carbon-carbon double bonds contribute somewhat more to compound adsorption on alumina as compared to silica gel, and hence compounds with unsaturation are generally better separated on Alumina than on other polar adsorbents such as silica gel. Alumina manufactured is of three types based on the pH ranges – acid, neutral and basic.

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Morphology Control of Phase-Separation-Induced Alumina−Silica …

Phase-separation behavior in the sol−gel system of alumina−silica (Al 2 O 3 −SiO 2) in the presence of poly (ethylene oxide) has been investigated.Amorphous gels with interconnected macropores can be obtained from the starting composition containing up to 10 mol % Al 3+ by inducing phase separation parallel to the sol−gel transition. SmCl 3 ·6H 2 O is …

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Removing Silica and Alumina from Limonite Using Wet High …

Removing alumina and silica from the limonite by wet high gradient magnetic separator was conducted to elevate iron grade of limonite which is based on the investigation of mineralogy of the ore. The results show that alumina exists mainly in the form of kaolinite and silica exists mainly in silicate, which mainly occurs with a size below 0.074 mm.

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2.3D: Separation Theory

In this section are discussed the details of the separation. TLC is an excellent analytical tool for separating mixtures in a sample. In this section are discussed the details of the separation. ... the stationary phase is a silica or alumina adsorbent and the mobile phase is an organic solvent or solvent mixture (the "eluent") that rises up ...

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